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Dionex Integrion HPIC system

MANUFACTURER ThermoFisher scientific
CONTACT 1 Pamela Moderate
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Description

This system performs versatile and efficient analyses through comprehensive application solutions and interactive wellness features. The Dionex Integrion system's flexible detector configurations meet your analysis needs for today and tomorrow. Its high-pressure capabilities enable faster analysis without compromising data quality. Use the system's automated eluent generation (EG) to eliminate error-prone manual eluent preparation and achieve better method reproducibility.

Specification

Pump Type Isocratic, dual-piston (in series), microprocessor-controlled, constant-stroke, variable-speed, patented Isokinetic Eluent Precompression

Construction Chemically inert, metal-free PEEK pump heads and flow path; compatible with aqueous eluents from pH 0–14 and reversed-phase solvents

Pressure Range 0–41 MPa (0–6000 psi)

Flow Rate Range Flow Rate Range: 0.001–22.4* mL/min with settable flow increments at 0.001 mL/min

  • Flow rates above 10 mL/min require optional high flow rate pump heads

Flow Rate Precision < 0.1%

Flow Rate Accuracy 0.1%

Pressure Ripple <1.00% at 1.0 mL/min

Reservoir Pressure None required; optional regulator assembly available

Vacuum Degasser Option, low-pressure

Pump Seal Wash Option, automatic operation

RFIC-EG Gradients Electrolytic eluent generation at high pressure 0.1–100 mM

Gradient Profiles Any combination of an unlimited number of linear, convex, and concave positive and negative gradient profiles

Eluent Shutoff Valve Electrically-actuated

Leak Sensor Built-in, optical A Specifications 222 Dionex Integrion Operator’s Manual Thermo Scientific Eluent Generator

Eluent Concentration Range 0.1–100 mM Concentration increments are 0.01 mM

Flow Rates 0.1–3.0 mL/min 1.0 mL/min eluent concentration is limited Eluent Types (Standard Pressure) Potassium hydroxide, lithium hydroxide, sodium hydroxide, potassium carbonate, carbonate/bicarbonate, methanesulfonic acid

Eluent Types (High Pressure) Potassium hydroxide, potassium carbonate, carbonate/bicarbonate, methanesulfonic acid

Maximum Operating Pressure 35 MPa (5000 psi)

Maximum Solvent Concentration Cations: None Anions: 25% methanol

Gradient Profiles Any combination of an unlimited number of linear, convex, and concave positive and negative gradient profiles

Number of Cartridges Supported Two

Heated Column Compartment Temperature Range 30–80 °C Minimum temperature: 5 °C above ambient) Equilibration time (ambient to ambient plus °20 C): 20 min

Temperature Accuracy ±0.5 °C (at 30°C)

Temperature Stability ±0.2 °C (at 30°C)

Temperature-Controlled Detector Compartment Temperature Range 15–40 °C Minimum temperature: 15 °C or 20 °C below ambient (whichever is higher) Equilibration time (ambient to ambient minus °20 C): 30 min

Temperature Accuracy ±0.5 °C (at 15 °C)

Temperature Stability ±0.2 °C (at 15 °C)

Suppression Modes Electrolytic Suppression, Self-Regenerating, Recycle Mode

Electrolytic Suppression, Self-Regenerating, External Water Mode

Non-Suppressed Conductivity Supported (both anion and cation) A Specifications

Chemical Suppression 2 mm and 4 mm anion and cation, membrane suppression bed type

Displacement Chemical Regeneration 2 mm and 4 mm anion and cation, membrane suppression bed type

Conductivity Detector Electronics Type Microprocessor-controlled digital signal processing, autoranging

Cell Drive 8 kHz square wave

Linearity 1%

Resolution 0.00238 nS/cm

Output Range Digital signal range: 0–15,000 S/cm Analog signal range: 0–15,000 S/cm

Noise, Wet < 0.2 nS at 23 S/cm background < 0.1 nS at 1 S/cm background

Filter Rise times 0 to 10 s, programmable

Sampling Rate 1 to 100 Hz, user-settable or automatic

Cell Temperature 7 °C above ambient to 60 °C maximum; user-settable working range is identical to settable range

Cell Temperature Stability < 0.001 °C

Cell Temperature Compensation Default 1.7% per °C; programmable from 0–3% per °C

Flow Cell Maximum Pressure 10 MPa (1500 psi)

Flow Cell Volume 0.7 L

Cell Electrodes Passivated 316 stainless steel, compatible with MSA

Cell Body Chemically inert polymer

Heat Exchanger Inert, tortuous-path for low axial dispersion

Electrochemical Detector Electronics Type Microprocessor-controlled digital signal processing

Electronic Noise (Wet Noise) IPAD (Au electrode) < 50 pC at 10 mM KOH DC Amperometry (GC) < 10 pA at catecholamine eluent

Potential Range -2.0 to 2.0 V in 0.001 V increments Suppression Modes, continued A Specifications 224 Dionex Integrion Operator’s Manual Thermo Scientific

Signal Range (Digital and Analog) Integrated Amperometry: 50 pC to 200 C DC Amperometry: 5 pA to 74 A

Filter 0–10 s response time, user-settable

Control Mode Local or remote control using relay closures or TTL, or control using Chromeleon software

Cell Body Titanium body with titanium inlet tubing Compatible with 2–7 mm ID columns

Working Electrodes Conventional: Gold, glassy carbon, platinum, and silver Disposable: Gold, platinum, carbon, and silver

Reference Electrodes pH-Ag/AgCl combination, one-piece design PdH, one-piece design

Autoranging Yes

Analog Output User-selectable full scale of 10, 100, or 1000 mV

Cell Volume at Working Electrode < 0.2 L

Maximum Cell Operating Pressure 0.7 MPa (100 psi)

System Software Chromeleon Chromatography Data System

Physical Specifications Power Requirements 100–240 Vac, 5 A, 50-60 Hz autoranging

Operating Temperature 4–40 °C (40–104 °F); cold-room compatible (4 °C) as long as system power remains on

Operating Humidity Range 20–80% relative, noncondensing

Control Modes Full control through Chromeleon software and optional Dionex Integrion Mobile App; alternative control through TTL or relay closures; two relay outputs, two TTL outputs, four programmable inputs

USB Communication Protocol One USB input; one built-in two-output USB hub

Dimensions (h × w × d) 62. 5 x 30 x 55.9 cm (24.6 x 11.8 x 22 in)

Weight 41 kg (90 lb)

Item ID #1584.

Last Updated: 10th April, 2017